May 1, 2008 By:
Ian J. Garrard, Derek Fisher, Ian A. Sutherland

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The authors discuss a preparative process using the principles of countercurrent chromatography. This process is faster, capable of loadings from milligrams to hundreds of grams, and uses robust equipment.

Dec 1, 2007 By:
Ronald E. Majors

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In this month?s installment, columnist Ron Majors covers the field of immunoextraction, a technique that employs immobilized antibodies to selectively capture specific analytes using molecular recognition via antibody?antigen interactions. Recently, the introduction of commercial products for specific high-volume environmental and food safety applications has spurred further applications of this technique.

May 1, 2007 By:
Ronald E. Majors

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This month's installment of "Sample Prep Perspectives" describes a new extraction technique called QuEChERS (standing for quick, easy, cheap, effective, and safe and is pronounced "catchers") for the sample preparation of pesticides in foods and agricultural samples.

Feb 1, 2007 By:
Ronald E. Majors, Nina Zolotarjova, Peter Mrozinski

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This installment of "Sample Prep Perspectives" discusses techniques for the reduction/depletion of high-abundance proteins.

Jan 1, 2007 By:
Ronald E. Majors

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Although the majority of solid-phase extraction (SPE) is performed with conventional bonded silica- and polymeric-phases, difficult and complex samples may require more specialized stationary phases. In this installment of "Sample Prep Perspectives," columnist Ron Majors discusses advanced topics such as multimodal SPE, restricted-access media, molecular imprinted polymers, immunoaffinity extraction phases, and other class- or compound-specific sorbents. These phases provide additional selectivity, and procedures using them can be automated. Representative applications will be presented.


Jul 1, 2006 By:
Ronald E. Majors

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In this installment of "Sample Prep Perspectives," Ron Majors examines modern sample preparation methods for solids that often involve increased temperature and higher pressure to speed up the extraction process.

Jul 1, 2006 By:
Luke Chimuka, Ewa Cukrowska
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Commercialization of the passive sampler is very important because it reflects acceptance by the wider community.

Jun 1, 2006 By:
Luke Chimuka, Ewa Cukrowska

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Guest authors Luke Chimuka and Ewa Cukrowska provide an in-depth look at the verious approaches to passive sampling, weighing the merits and challenges for each type.
